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Beilstein J. Org. Chem. 2023, 19, 36–56, doi:10.3762/bjoc.19.4
Graphical Abstract
Figure 1: Training set of tri- and tetracoordinate phosphorus compounds; chemical shifts are in ppm, referenc...
Figure 2: (a) Plot of experimental vs calculated chemical shifts of tri- and tetracoordinate phosphorus compo...
Figure 3: Plot of experimental vs calculated chemical shifts of training set compounds reported by Latypov et...
Figure 4: “Large” compounds selected for 31P NMR calculation by Latypov [37].
Figure 5: Stereoisomers and unusual phosphorus compounds used for chemical shift calculations.
Figure 6: Phosphorus-catalyzed oxygen transfer reaction intermediates.
Figure 7: Phosphirane reactions.
Figure 8: (a) Plot of experimental vs scaled chemical shifts derived from the tri- and tetracoordinate phosph...
Beilstein J. Org. Chem. 2015, 11, 184–191, doi:10.3762/bjoc.11.19
Figure 1: Acyl phosphorus compounds.
Scheme 1: Synthesis of a dinucleoside acylphosphonate (3b) and a formate diester (1a).
Scheme 2: Reaction of an H-phosphonodiamidite with acid chlorides.
Figure 2: ORTEP [52] drawing of 9. Selected distances (Å) and angles (°): P–N1 1.687(1), P–N2 1.679(1), P–C1 1.87...
Scheme 3: Synthesis of dinucleosides.
Scheme 4: Calculated phosphine, acylphosphine, phosphite, and acylphosphonite inversion barriers.